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By the Authority Vested By Part 5 of the United States Code § (a) and. Part 1 of the Code of Regulations § 51 the attached document has been duly. AppNote the analysis of sulfur in bunker fuel and diesel as per ASTM D is demonstrated This standard is issued under the fixed designation D ; the number immediately 1 This test method is under the jurisdiction of ASTM Committee D02 on.

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D Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy- Dispersive X-ray Fluorescence Spectrometry 1 This standard is issued under the fixed designation D ; the number immediately following the designation indicates the year of original adoption or, in the case of revision, the year of last revision.

Therefore, it is critical to monitor the sulfur content to ensure regulatory compliance and to improve air quality, affecting those utilizing as well as producing and supplying bunker fuels. A number in parentheses indicates the year of last reapproval.

Sulfur in bunker fuel by ASTM D4294

Therefore, the Std 6 0. Samples that are diluted can have higher errors than indicated in Section 16 than non-diluted samples. Click here to sign up. In these cases, other materials interference is greatest if the water creates a layer over the transparent film as it will attenuate the X-ray intensity for sulfur. Samples that are diluted can have higher errors than indicated in Section 16 than non-diluted samples. Oxygenated fuels with ethanol or methanol contents exceeding the limits given in Table 1 can be dealt with using this test method, but the precision and bias statements do not apply see Appendix X3.

As soon as any sedlffient or Method D or any other equivalent low level sulfur change d494 concentration is observed, discard the standard. Thus, a gasoline may be simulated by 7.

Active view current version of standard. Criminal penalties may apply for noncompliance. This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and if not revised, either reapproved or withdrawn: Once aU “the on the criticality of the quality being measured and the standards have been analyzed, follow the manufacturer’s demonstrated stability of the testing process, the frequency of instructions for generating the optimum calibration curve based quality control sample testing can range from.

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Significance and Use 1. For specific significantly different composition than the white oil calibra- precautionary statements, see Section 7.

Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. Knowledge of sulfur concentration is 0. Aliy out of control asfm shall recommended counting time for the instrument according to trigger investigation for root cause s. No other units of measurement are included in this standard.

These variations directly influence I This test method is under the jurisdiction of Committee D-2 on Petroleum X-ray absorption and change the measured intensity of each Products and Lubricants and is the direct responsibility of Subcommittee D An estimate of the limit of detection is three times the reproducibility standard deviation, and an estimate of the limit of quantitation is ten times the reproducibility standard deviation.

It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Generally speaking, filling the sample cup to at 5. Depending prepared cells and fresh portions of the standard. Results are recorded volves setting up the instrument for recording of net sulfur a. White mineral be used in place of some or all of the standards prescribed in oil see 7.

The measured’ as in 9. There may be a loss of sensitivity and precision. Therefore, it is essential that the film Range 2 be taut and clean to ensure reliable results.

Users of this standard are expressly advised that determination of the validity of any such f4294 rights, and the risk of infringement of such rights, are entirely their own responsibility. Corrections should Analytical Reagents of the American Chemical Society where be verified for new formulations. Calibration and Standardization 9. Referenced Documents interpreting the results.

Link to Active This link will always route to the current Active version of the standard. Provide a vent hole in the top to prevent bowing.

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SECAs are defined protected areas in which only low sulfur bunker fuels and marine diesels can be used. A new piece 6.

Sulfur in bunker fuel by ASTM D | Rigaku

Unless otherwise indicated, it is intended that to time and that the software corrections offered by the all reagents conform to the specifications of the Committee on manufacturer not be accepted at face value.

Obtain the average A gas filled proportional fingerprints can affect the reading when analyzing for low counter has been found to be suitable to use. Note 1—Oxygenated fuels with ethanol or methanol contents exceeding the limits given in Table 1 can be dealt with using this test method, but the precision and bias statements do not apply see Appendix X3. Oil from resolution value not to exceed eV.

Background Sulfur content is regulated in many petroleum fuels oils,and plays an important role in fuel quality and control of polluting emissions. These materials can include diesel fuel, jet fuel, kerosine, other distillate oil, naphtha, residual oil, lubricating base oil, hydraulic oil, crude oil, unleaded gasoline, gasoline-ethanol blends, biodiesel see Note 2and similar petroleum products.

Link to Active This link will always route to the current Active version of the standard.

It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Read more about nano3DX Astj Popular products by category.

Non-destructively analyze from sodium Na through uranium U in almost any matrix, from solids and alloys to powders, liquids and slurries. However, Samples should be analyzed immediately after pouring into a attention to the source is only to be carried out by a fully trained and competent person using the correct shielding techniques. These types of interferences are always present in intensity into percent sulfur concentration. Desktop Site Mobile Site. Analytical solutions by industry.

Use the certified sulfur the sample.

The calculated to four decimal places.